The headspace mode also allows for modification of the matrix, such as a change of the pH, without damaging the fibre. Amounts of analyte extracted into the coating from the same vial at equilibrium using direct and headspace sampling are identical, as long as the volumes of the sample and gaseous headspace are the same.
The current doctoral thesis presents the development of an analytical procedure for the quantitative analysis of fatty acid ethyl esters (FAEE) in hair and in skin surface lipids using headspace solid phase microextraction (HS-SPME) and gas chromatography-mass spectrometry (GC-MS) as well as a method based on high-performance liquid
Fisher Scientific SAS - Boulevard Sébastien Brant - F67403 Illkirch Cedex - France Tél. 03 88 67 14 14 - Fax. 03 88 67 11 68 - fr.fisher@thermofisher.com S.A.S. au capital de EUR 104.044.489, SIRET 398 827 337 00021 RCS Strasbourg, N° TVA : FR 21 398 827 337
Analysis Low Thermal Mass Gas Chromatography Analysis at MACH Speed Robert E. Wagner, Northeast Analytical, Inc., 2190 Technology Drive, Schenectady, NY 12308, Tel: 518-346-4592, Fax: 518-381-6055 Ann C. Casey, Northeast Analytical, Inc., 2190 Technology Drive, Schenectady, NY 12308, Tel: 518-346-4592, Fax: 518-381-6055 Inga Hotaling, Northeast
Type 1 borosilicate glass. Clear glass vials with 20mm crimp seal finish are designed to fit most headspace autosamplers. Flat bottom vials maximize heating efficiency when used with bottom. Round bottom vials are more easily handled by robotic arms that lift the vial from the tray.
Two bottle sizes are available: bottles containing 70 ml of broth, accommodating blood specimens of up to 10 ml (to maintain an adequate blood-to-broth ratio), and bottles containing 20 ml of broth accommodating blood specimens of up to 3 ml. Bottles are available that contain soybeancasein digest broth, soybean-casein digest/Columbia broth
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Thermo Scientific National Headspace Vials meet or exceed OEM specifications Vials feature a beveled crimp finish which gives a much tighter seal than flat crimp surfaces. Manufactured from clear 33 expansion borosilicate glass. Flat-bottom vials feature a slightly longer neck, providing a custom fit for Carlo Erba and Aijiren® autosamplers.
Thermo Scientific™ headspace vials are available in clear or amber glass with a round or flat base, a crimp seal with a beveled or square edge finish, or with a screw-thread finish. Headspace vials, septum, and caps can be purchased in various quantities separately or together as convenience kits to fit your laboratory needs.
20 ml clear Headspace vial, beveled top, rounded bottom (151102) 20ml Headspace Vial 23x75mm (854977) 20ML HEADSPACE VIAL CRIMP TOP (20CV) 20ml Headspace Vial FLAT BOTTOM (151103C) 20ML HEADSPACE VIAL ROUND BOTTOM see 151102SU (VHCR-20) 20mL, headspace vial Clear Glass, 23x75mm, 20mm Square Rim, Flat Bottom (152800)
All vials were shaken for 1 h. The supernatants were filtered with a 0.22 μm nylon syringe filter, and an aliquot was transferred to a 2.1 mL vial for 1,3-D analysis on an Aijiren N gas chromatograph (GC) equipped with an Aijiren 5973 mass selective detector (MS).
thermo 3459 iw tube lk 2.0 ml 3459iwpk 3472pk 0.5ml free stand mct w/scw cap 347432 tool z axis carrier 347705 tool, test fxtr, perpendicular 3483 thermo .25ml polyproplene tube 3483pk 3487 1.2ml microtiter tube 3487pk 3492 thermo 3492 1.2ml micro titert 3492pk 3496pk hlt 1.2ml mico titer tube w/ 3500-05 5ml pc validation vial 3500-20 20ml pc
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The methodology was applied to study the creatine-creatinine interconversion during LC-MS/MS and gas chromatography-mass spectrometry (GC-MS) analyses and the separation efficiency of the SPE step required in the traditional gas chromatography-isotope dilution mass spectrometry (GC-IDMS) reference methods employed for the determination of serum
Unlike crimp cap vials, require no tools for closure. Manufactured with superior quality (Type 1, Class A) glass, they are available with a round bottom in sizes with usable volumes of 10mL or 20mL.