The Role of Vial Inserts in Minimizing Sample Contamination in Autosamplers

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Placing Vials and Bottles in the Sampler 118 Using Two Injectors ( , only) 121 How Many Sample Vials Can I Run? 122 Solvent bottle equation (G2913 A injector) 123 Waste bottle equation 123 Example 124 Reduced solvent and sample usage 127 7 Running Samples Running a Sample 130 Using the ALS Controller 131 Interrupting A Run Or Sequence

The amount of sample available for analysis is important in choosing the appropriate vial. If only a limited volume of sample is available, you will have to choose between using an insert for your regular autosampler vial, a microvial or a high recovery vial.

Jun 20, 2023 · HPLC inserts play a crucial role in preserving the sample integrity by minimizing the contact between the sample and the vial surface. This prevents analyte adsorption, degradation, and contamination, ensuring reliable and consistent results.

The “acidic” functionality of silanols has been known to cause adsorption of basic compounds, change the sample solution pH and/or hydrolyze susceptible compounds rendering them undetectable. With RSA™ Glass vials and inserts there is virtually no sample “loss to the vial” and no “pH shifting” making your analysis data more reliable.

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Autosampler Vials Thermo Scientific™ 9mm Clear Glass Screw Thread Vials Nearly eliminate septa push-through and improve sealing with vials built with the innovative Advanced Vial Closure System (AVCS).

All autosamplers aspirate a sample from a vial or well plate. Differences arise in sample placement inside the sample loop and the relationship of the needle to the mobile phase flow path. There are two main autosampler operating principles: pushed/pulled-loop and split-loop.

PTFE Vial Support Sleeve for 7x32mm vials, fits most autosamplers PTFE No 12x32 Flat Bottom – – – WS-5 40 Sleeves adapt 6x32mm vials for use in autosamplers designed for 12x32mm vials. Use sleeve SV-S1 for autosamplers that do not lift the vial from the tray. Use SV-S11A or SV-S11G for autosamplers that move the vial during sampling.

3. Sample carryover - demonstrated when an injection of a solvent blank produces a replicated version of the previous sample's chromatogram, just on a smaller scale. Most of the time, it occurs as a result of adsorption of the analyte within the injection component . Common contamination issues. 1.

Jul 31, 2020 · 1. Increased Precision and Accuracy. HPLC inserts feature precise designs and dimensions to provide accurate and reproducible results, while micro vial inserts minimize sample loss during injection for precise quantitative analysis. Their tight-fitting nature means minimal sample loss during injection and ensures all sample volume reaches the

ing to minimize sample temperatures, hexane probably is the most volatile solvent that chromatographers can use successfully and consistently. Back-loading autosamplers: In a back-loading autosampler, a second dedicated sampling needle removes liquid from the sample vials and solvent reservoirs. Instead of depending upon syringe plunger suction,

vials and closures from microsampling to headspace to match popular application requirements. Vial choices include: Crimp Top, Snap Top, and Screw top vials with a selection of closures. Refer to the Autosampler Compatibility Table on pages 10-11 to determine which vials, closures and inserts will work on your specific autosampler unit.

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