May 01, 2020 · Extracts were stored in three types of vials: 2-mL screw cap gas chromatography (GC) vials, 2-mL crimp cap GC vials, and 4-mL screw cap vials. To evaluate persistence, c-strips were stored at room temperature then eluted at multiple time intervals: 0 days (immediately following extraction), 10 days, 1 month, 6 months, 1 year, and 2 years.
and sealed into a 10 mL crimp cap headspace vial (vials P/N 10CV, caps P/N 20-MCBC-ST3). As specified in the EN 13628-1:2002 method, the ratio between the sample area (in cm2) and the vial volume (in mL) was maintained between 3 and 5.
7. Transfer back section with remaining glass wool plugs to a second vial. 8. Add 1.0 mL toluene to each vial. Crimp cap tightly onto each vial. NOTE: An appropriate internal standard, such as 1 µL/mL dimethylformamide, may be added at this point [3]. 9. Agitate vials in an ultrasonic water bath for 60 min. CALIBRATION AND QUALITY CONTROL: 10.
GC-MS/MS 2. Add to the headspace vial 9980 µL of water or fill up to the mark on the volumetric flask 1. Weigh 100 mg of homogenized sample to the headspace vial or volumetric flask 3. Add to the sample 2.5 g of NaCl 4. T ig h t ly ca p ev w n osur with Butyl/PTFE septa 5. Place the vial to the Autosampler of GC-MS/MS 6. Automatic SPME process
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5.2.3.4 Sample vials: Amber glass, 1- to 3-mL with PTFE-lined screw- or crimp-cap, to fit GC autosampler. 5.3 Gas Chromatograph (GC): Analytical system with split injection, capillary column,
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ing known volumes (3–30 mL) of a standard solu-tion in water, having the composition reported in Table 1, to 3.0g of cotton wool, together with 86 mg of crotonic acid (IS) in a 20-mL HS clear glass vial with a silicone/PTFE crimp cap (Supelco, Belle-fonte). Then it was subjected to a HS-SPME pro-cedure. The GC-MS chromatogram was collected
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