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Volatile organic contaminants (VOCs) were detected by the application of HS-SPME-GCMS. Samples were prepared by adding 10 mL of sample water to 20 mL amber vials resulting in 10 mL of head space. Next, vials were agitated at 50 °C and 500 rpm alternating direction every 10 s for 30 min.
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Mar 31, 2017 · Gas Chromatography—Mass Spectrometry (GC/MS) Empty glass vials were stored at 60°C for 2–3 days, and then removed from a dryer and left to stand for about 15 minutes to equilibrate with the surroundings. 2 g of the bacterial pellet from OPTION 2 was weighed, transferred into a vial and capped.
Aug 09, 2016 · USDA Lehotay ITSP QuEChERS Chromatographia-2016 1. 1 3 DOI 10.1007/s10337-016-3116-y Chromatographia ORIGINAL Automated Mini‑Column Solid‑Phase Extraction Cleanup for High‑Throughput Analysis of Chemical Contaminants in Foods by Low‑Pressure Gas Chromatography—Tandem Mass Spectrometry Steven J. Lehotay1 · Lijun Han1,2 · Yelena Sapozhnikova1 Received: 8 April 2016 / Accepted: 24 May
Fast low-pressure gas chromatography tandem mass spectrometry (LPGC-MS/MS) and liquid chromatography (LC)-MS/MS were used for analysis. The QuEChERS AOAC Official Method 2007.01 was also tested